Carbonic anhydrase inhibitors: DNA cloning and inhibition studies of the alpha-carbonic anhydrase from Helicobacter pylori, a new target for developing sulfonamide and sulfamate gastric drugs.

Article Details

Citation

Nishimori I, Minakuchi T, Morimoto K, Sano S, Onishi S, Takeuchi H, Vullo D, Scozzafava A, Supuran CT

Carbonic anhydrase inhibitors: DNA cloning and inhibition studies of the alpha-carbonic anhydrase from Helicobacter pylori, a new target for developing sulfonamide and sulfamate gastric drugs.

J Med Chem. 2006 Mar 23;49(6):2117-26.

PubMed ID
16539401 [ View in PubMed
]
Abstract

We have cloned and sequenced Helicobacter pylori alpha-class carbonic anhydrase (hpCA) from patients with different gastric mucosal lesions, including gastritis (n=15), ulcer (n=6), and cancer (n=16). Although several polymorphisms were newly identified such as 12Ala, 13Thr, 16Ile, and 168Phe, there was no significant relevance of any polymorphism with gastric mucosal lesion types. A library of sulfonamides/sulfamates has been investigated for the inhibition of hpCA, whereas new derivatives have been obtained by attaching 4-tert-butyl-phenylcarboxamido/sulfonamido tails to benzenesulfonamide/1,3,4-thiadiazole-2-sulfonamide scaffolds. All types of activity for inhibition of hpCA have been detected. Dorzolamide and simple 4-substituted benzenesulfonamides were weak inhibitors (KI 873-4360 nM). Sulfanilamide, orthanilamide, some of their derivatives, and indisulam showed better activity (KI 413-640 nM), whereas most of the clinically used inhibitors, such as methazolamide, ethoxzolamide, dichlorophenamide, brinzolamide, topiramate, zonisamide, etc., acted as medium-potency inhibitors (KI 105-378 nM). Some potent hpCA inhibitors were detected too (KI 12-84 nM) among acetazolamide, 4-amino-6-chloro-1,3-benzenedisulfonamide and some newly designed compounds incorporating lipophilic tails. Some of the newly prepared derivatives had selectivity ratios for inhibiting hpCA over hCA II in the range of 1.25-3.48, showing thus some selectivity for inhibiting the bacterial enzyme. Since hpCA is essential for the survival of the pathogen in acid, it might be used as a new pharmacologic tool in the management of drug-resistant H. pylori.

DrugBank Data that Cites this Article

Binding Properties
DrugTargetPropertyMeasurementpHTemperature (°C)
4-(2-AMINOETHYL)BENZENESULFONAMIDECarbonic anhydrase 2Ki (nM)1607.525Details
5-(2-chlorophenyl)-1,3,4-thiadiazole-2-sulfonamideCarbonic anhydrase 2Ki (nM)127.525Details
5-[(phenylsulfonyl)amino]-1,3,4-thiadiazole-2-sulfonamideCarbonic anhydrase 2Ki (nM)97.525Details
6-HYDROXY-1,3-BENZOTHIAZOLE-2-SULFONAMIDECarbonic anhydrase 2Ki (nM)307.525Details
AcetazolamideCarbonic anhydrase 1Ki (nM)2507.525Details
AcetazolamideCarbonic anhydrase 2Ki (nM)127.525Details
BrinzolamideCarbonic anhydrase 1Ki (nM)450007.525Details
BrinzolamideCarbonic anhydrase 2Ki (nM)37.525Details
DiclofenamideCarbonic anhydrase 1Ki (nM)12007.525Details
DiclofenamideCarbonic anhydrase 2Ki (nM)387.525Details
DorzolamideCarbonic anhydrase 1Ki (nM)500007.525Details
DorzolamideCarbonic anhydrase 2Ki (nM)97.525Details
EthoxzolamideCarbonic anhydrase 1Ki (nM)257.525Details
EthoxzolamideCarbonic anhydrase 2Ki (nM)87.525Details
MethazolamideCarbonic anhydrase 1Ki (nM)507.525Details
MethazolamideCarbonic anhydrase 2Ki (nM)147.525Details
TopiramateCarbonic anhydrase 1Ki (nM)2507.525Details
TopiramateCarbonic anhydrase 2Ki (nM)107.525Details
ZonisamideCarbonic anhydrase 1Ki (nM)567.525Details
ZonisamideCarbonic anhydrase 2Ki (nM)357.525Details