Carbonic anhydrase inhibitors: clash with Ala65 as a means for designing inhibitors with low affinity for the ubiquitous isozyme II, exemplified by the crystal structure of the topiramate sulfamide analogue.

Article Details

Citation

Winum JY, Temperini C, El Cheikh K, Innocenti A, Vullo D, Ciattini S, Montero JL, Scozzafava A, Supuran CT

Carbonic anhydrase inhibitors: clash with Ala65 as a means for designing inhibitors with low affinity for the ubiquitous isozyme II, exemplified by the crystal structure of the topiramate sulfamide analogue.

J Med Chem. 2006 Nov 30;49(24):7024-31.

PubMed ID
17125255 [ View in PubMed
]
Abstract

The sulfamide analogue of the antiepileptic drug topiramate is a 210 times less potent inhibitor of isozyme II of the zinc enzyme carbonic anhydrase (CA, EC 4.2.1.1) compared to topiramate but effectively inhibits isozymes CA VA, VB, VII, XIII, and XIV (KI in the range of 21-35 nM). Its weak binding to CA II is due to a clash between one methyl group of the inhibitor and Ala65 and may be exploited for the drug design of compounds with lower affinity for this ubiquitous isozyme, as Ala65 is unique to CA II. As shown by X-ray crystallography, the sulfamide analogue binds to CA II with the deprotonated sulfamide moiety coordinated to Zn(II) and with the organic scaffold making an extended network of hydrogen bonds with Thr199, Gln92, His94, Asn62, and Thr200. Its binding to this isozyme is more similar to that of topiramate and quite different from that of the topiramate cyclic sulfate analogue RWJ-37947.

DrugBank Data that Cites this Article

Polypeptides
NameUniProt ID
Carbonic anhydrase 2P00918Details
Binding Properties
DrugTargetPropertyMeasurementpHTemperature (°C)
AcetazolamideCarbonic anhydrase 1Ki (nM)2507.522Details
AcetazolamideCarbonic anhydrase 12Ki (nM)5.77.522Details
AcetazolamideCarbonic anhydrase 14Ki (nM)417.522Details
AcetazolamideCarbonic anhydrase 2Ki (nM)127.522Details
AcetazolamideCarbonic anhydrase 4Ki (nM)747.522Details
AcetazolamideCarbonic anhydrase 7Ki (nM)2.57.522Details
DiclofenamideCarbonic anhydrase 1Ki (nM)12007.522Details
DiclofenamideCarbonic anhydrase 2Ki (nM)387.522Details
DiclofenamideCarbonic anhydrase 4Ki (nM)150007.522Details
DiclofenamideCarbonic anhydrase 7Ki (nM)267.522Details
DorzolamideCarbonic anhydrase 1Ki (nM)500007.522Details
DorzolamideCarbonic anhydrase 2Ki (nM)97.522Details
DorzolamideCarbonic anhydrase 4Ki (nM)85007.522Details
EthoxzolamideCarbonic anhydrase 1Ki (nM)257.522Details
EthoxzolamideCarbonic anhydrase 2Ki (nM)87.522Details
EthoxzolamideCarbonic anhydrase 4Ki (nM)937.522Details
EthoxzolamideCarbonic anhydrase 7Ki (nM)0.87.522Details
MethazolamideCarbonic anhydrase 1Ki (nM)507.522Details
MethazolamideCarbonic anhydrase 2Ki (nM)147.522Details
MethazolamideCarbonic anhydrase 4Ki (nM)62007.522Details
MethazolamideCarbonic anhydrase 7Ki (nM)2.17.522Details
Sulfamic Acid 2,3-O-(1-Methylethylidene)-4,5-O-Sulfonyl-Beta-Fructopyranose EsterCarbonic anhydrase 2Ki (nM)367.522Details
TopiramateCarbonic anhydrase 1Ki (nM)2507.522Details
TopiramateCarbonic anhydrase 2Ki (nM)107.522Details
TopiramateCarbonic anhydrase 4Ki (nM)49007.522Details